| Refinement on F2 | Hydrogen site location: inferred from neighbouring sites |
| Least-squares matrix: full | H-atom parameters constrained |
| R[F2 > 2σ(F2)] = 0.041 | w = 1/[σ2(F2) + (0.04P)2 + 0.59P], where P = [max(Fo2,0) + 2Fc2]/3 |
| wR(F2) = 0.098 | (Δ/σ)max = 0.0001 |
| S = 0.93 | Δρmax = 0.32 e Å−3 |
| 1528 reflections | Δρmin = −0.33 e Å−3 |
| 172 parameters | Extinction correction: None |
| Primary atom site location: structure-invariant direct methods |