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. 2008 Nov 13;64(Pt 12):m1539. doi: 10.1107/S160053680803417X
Rigaku Mercury2 diffractometer 2629 independent reflections
Radiation source: fine-focus sealed tube 1952 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.057
Detector resolution: 13.6612 pixels mm-1 θmax = 27.5º
T = 293(2) K θmin = 3.1º
ω scans h = −12→12
Absorption correction: multi-scan(CrystalClear; Rigaku, 2005) k = −14→14
Tmin = 0.909, Tmax = 1.000 l = −14→14
11307 measured reflections