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. 2008 Nov 8;64(Pt 12):m1504. doi: 10.1107/S1600536808035253
Rigaku Mercury diffractometer 16405 independent reflections
Radiation source: fine-focus sealed tube 10865 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.096
T = 293(2) K θmax = 25.4º
ω scans θmin = 3.1º
Absorption correction: multi-scan(Jacobson, 1998) h = −14→16
Tmin = 0.782, Tmax = 0.847 k = −21→21
44634 measured reflections l = −22→24