| Rigaku Mercury diffractometer | 16405 independent reflections |
| Radiation source: fine-focus sealed tube | 10865 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.096 |
| T = 293(2) K | θmax = 25.4º |
| ω scans | θmin = 3.1º |
| Absorption correction: multi-scan(Jacobson, 1998) | h = −14→16 |
| Tmin = 0.782, Tmax = 0.847 | k = −21→21 |
| 44634 measured reflections | l = −22→24 |