Bruker P4 diffractometer | Rint = 0.049 |
Radiation source: fine-focus sealed tube | θmax = 25.0º |
Monochromator: graphite | θmin = 1.8º |
T = 295(2) K | h = −23→1 |
θ/2θ scans | k = −1→27 |
Absorption correction: ψ scan(XSCANS; Siemens, 1996) | l = −1→15 |
Tmin = 0.905, Tmax = 0.929 | 3 standard reflections |
3430 measured reflections | every 97 reflections |
2824 independent reflections | intensity decay: none |
1980 reflections with I > 2σ(I) |