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. 2008 Nov 22;64(Pt 12):m1586. doi: 10.1107/S1600536808038154
Bruker P4 diffractometer Rint = 0.049
Radiation source: fine-focus sealed tube θmax = 25.0º
Monochromator: graphite θmin = 1.8º
T = 295(2) K h = −23→1
θ/2θ scans k = −1→27
Absorption correction: ψ scan(XSCANS; Siemens, 1996) l = −1→15
Tmin = 0.905, Tmax = 0.929 3 standard reflections
3430 measured reflections every 97 reflections
2824 independent reflections intensity decay: none
1980 reflections with I > 2σ(I)