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. 2008 Nov 13;64(Pt 12):o2339. doi: 10.1107/S1600536808035319
Rigaku Saturn CCD area-detector diffractometer 7730 independent reflections
Radiation source: rotating anode 6754 reflections with I > 2σ(I)
Monochromator: confocal Rint = 0.045
Detector resolution: 7.31 pixels mm-1 θmax = 27.5º
T = 113(2) K θmin = 1.5º
ω and φ scans h = −15→15
Absorption correction: multi-scan(CrystalClear; Rigaku/MSC, 2005) k = −12→11
Tmin = 0.976, Tmax = 0.988 l = −31→34
22853 measured reflections