Rigaku Saturn CCD area-detector diffractometer | 7730 independent reflections |
Radiation source: rotating anode | 6754 reflections with I > 2σ(I) |
Monochromator: confocal | Rint = 0.045 |
Detector resolution: 7.31 pixels mm-1 | θmax = 27.5º |
T = 113(2) K | θmin = 1.5º |
ω and φ scans | h = −15→15 |
Absorption correction: multi-scan(CrystalClear; Rigaku/MSC, 2005) | k = −12→11 |
Tmin = 0.976, Tmax = 0.988 | l = −31→34 |
22853 measured reflections |