Bruker SMART CCD area-detector diffractometer | 5479 independent reflections |
Radiation source: fine-focus sealed tube | 3677 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.023 |
T = 294(2) K | θmax = 25.0º |
phi and ω scans | θmin = 1.9º |
Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −10→8 |
Tmin = 0.945, Tmax = 0.968 | k = −13→10 |
8144 measured reflections | l = −18→18 |