| Rigaku R-AXIS RAPID IP diffractometer | 3595 independent reflections |
| Radiation source: fine-focus sealed tube | 2287 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.0000 |
| Detector resolution: 0.76 pixels mm-1 | θmax = 27.5º |
| T = 293(2) K | θmin = 2.3º |
| Oscillation scans | h = 0→11 |
| Absorption correction: empirical (using intensity measurements)(ABSCOR; Higashi, 1995) | k = −10→12 |
| Tmin = 0.805, Tmax = 0.992 | l = −13→13 |
| 3595 measured reflections |
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