| Bruker SMART 1000 CCD area-detector diffractometer | 2823 independent reflections |
| Radiation source: fine-focus sealed tube | 1566 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.027 |
| T = 298(2) K | θmax = 25.2º |
| ω scans | θmin = 1.3º |
| Absorption correction: multi-scan(SADABS; Bruker, 2001) | h = −19→18 |
| Tmin = 0.922, Tmax = 0.973 | k = −9→10 |
| 2956 measured reflections | l = −16→16 |
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