| Bruker APEX CCD diffractometer | 3102 independent reflections |
| Radiation source: fine-focus sealed tube | 2809 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.018 |
| T = 293(2) K | θmax = 26.0º |
| ω scans | θmin = 1.9º |
| Absorption correction: multi-scan(SADABS; Bruker, 1998) | h = −16→23 |
| Tmin = 0.691, Tmax = 0.732 | k = −18→17 |
| 8715 measured reflections | l = −16→17 |