C10—C9 | 1.521 (9) | N1—C17 | 1.341 (4) |
C10—H10A | 0.9600 | N1—C13 | 1.347 (4) |
C10—H10B | 0.9600 | N2—C22 | 1.333 (4) |
C10—H10C | 0.9600 | N2—C18 | 1.348 (4) |
C11—C9 | 1.519 (9) | C1—C2 | 1.505 (5) |
C11—H11A | 0.9600 | C2—C3 | 1.381 (5) |
C11—H11B | 0.9600 | C2—C7 | 1.386 (5) |
C11—H11C | 0.9600 | C3—C4 | 1.390 (5) |
C12—C9 | 1.501 (7) | C3—H3 | 0.9300 |
C12—H12A | 0.9600 | C4—C5 | 1.389 (5) |
C12—H12B | 0.9600 | C4—C8 | 1.502 (5) |
C12—H12C | 0.9600 | C5—C6 | 1.387 (5) |
C10'—C9 | 1.504 (8) | C5—H5 | 0.9300 |
C10'—H10D | 0.9600 | C6—C7 | 1.390 (5) |
C10'—H10E | 0.9600 | C6—C9 | 1.527 (6) |
C10'—H10F | 0.9600 | C7—H7 | 0.9300 |
C11'—C9 | 1.595 (9) | C8—Cu1ii | 2.538 (4) |
C11'—H11D | 0.9600 | C13—C14 | 1.368 (5) |
C11'—H11E | 0.9600 | C13—H13 | 0.9300 |
C11'—H11F | 0.9600 | C14—C15 | 1.365 (6) |
C12'—C9 | 1.502 (8) | C14—H14 | 0.9300 |
C12'—H12D | 0.9600 | C15—C16 | 1.382 (6) |
C12'—H12E | 0.9600 | C15—H15 | 0.9300 |
C12'—H12F | 0.9600 | C16—C17 | 1.373 (5) |
Cu1—O1 | 1.933 (2) | C16—H16 | 0.9300 |
Cu1—O3i | 1.956 (2) | C17—C18 | 1.477 (5) |
Cu1—N1 | 1.985 (3) | C18—C19 | 1.388 (5) |
Cu1—N2 | 1.983 (3) | C19—C20 | 1.376 (5) |
Cu1—C8i | 2.538 (4) | C19—H19 | 0.9300 |
O1—C1 | 1.273 (4) | C20—C21 | 1.377 (6) |
O2—C1 | 1.233 (5) | C20—H20 | 0.9300 |
O3—C8 | 1.279 (5) | C21—C22 | 1.372 (5) |
O3—Cu1ii | 1.956 (2) | C21—H21 | 0.9300 |
O4—C8 | 1.236 (4) | C22—H22 | 0.9300 |
C9—C10—H10A | 109.5 | C6—C5—C4 | 122.4 (3) |
C9—C10—H10B | 109.5 | C6—C5—H5 | 118.8 |
H10A—C10—H10B | 109.5 | C4—C5—H5 | 118.8 |
C9—C10—H10C | 109.5 | C5—C6—C7 | 116.8 (3) |
H10A—C10—H10C | 109.5 | C5—C6—C9 | 122.1 (3) |
H10B—C10—H10C | 109.5 | C7—C6—C9 | 121.0 (4) |
C9—C11—H11A | 109.5 | C2—C7—C6 | 121.8 (3) |
C9—C11—H11B | 109.5 | C2—C7—H7 | 119.1 |
H11A—C11—H11B | 109.5 | C6—C7—H7 | 119.1 |
C9—C11—H11C | 109.5 | O4—C8—O3 | 122.7 (3) |
H11A—C11—H11C | 109.5 | O4—C8—C4 | 119.8 (4) |
H11B—C11—H11C | 109.5 | O3—C8—C4 | 117.5 (3) |
C9—C12—H12A | 109.5 | O4—C8—Cu1ii | 76.6 (2) |
C9—C12—H12B | 109.5 | O3—C8—Cu1ii | 49.07 (17) |
H12A—C12—H12B | 109.5 | C4—C8—Cu1ii | 155.9 (2) |
C9—C12—H12C | 109.5 | C12—C9—C10' | 131.1 (4) |
H12A—C12—H12C | 109.5 | C12'—C9—C10' | 115.1 (5) |
H12B—C12—H12C | 109.5 | C12—C9—C11 | 108.0 (5) |
C9—C10'—H10D | 109.5 | C12'—C9—C11 | 132.1 (5) |
C9—C10'—H10E | 109.5 | C10'—C9—C11 | 58.7 (3) |
H10D—C10'—H10E | 109.5 | C12—C9—C10 | 111.7 (5) |
C9—C10'—H10F | 109.5 | C12'—C9—C10 | 78.2 (4) |
H10D—C10'—H10F | 109.5 | C10'—C9—C10 | 49.7 (2) |
H10E—C10'—H10F | 109.5 | C11—C9—C10 | 108.0 (4) |
C9—C11'—H11D | 109.5 | C12—C9—C6 | 112.9 (4) |
C9—C11'—H11E | 109.5 | C12'—C9—C6 | 113.5 (5) |
H11D—C11'—H11E | 109.5 | C10'—C9—C6 | 115.8 (4) |
C9—C11'—H11F | 109.5 | C11—C9—C6 | 110.0 (5) |
H11D—C11'—H11F | 109.5 | C10—C9—C6 | 106.1 (5) |
H11E—C11'—H11F | 109.5 | C12—C9—C11' | 67.9 (3) |
C9—C12'—H12D | 109.5 | C12'—C9—C11' | 102.3 (4) |
C9—C12'—H12E | 109.5 | C10'—C9—C11' | 103.9 (5) |
H12D—C12'—H12E | 109.5 | C11—C9—C11' | 47.3 (2) |
C9—C12'—H12F | 109.5 | C10—C9—C11' | 146.9 (5) |
H12D—C12'—H12F | 109.5 | C6—C9—C11' | 103.9 (5) |
H12E—C12'—H12F | 109.5 | N1—C13—C14 | 122.2 (4) |
O1—Cu1—O3i | 88.17 (11) | N1—C13—H13 | 118.9 |
O1—Cu1—N1 | 94.83 (11) | C14—C13—H13 | 118.9 |
O3i—Cu1—N1 | 172.79 (11) | C15—C14—C13 | 118.7 (4) |
O1—Cu1—N2 | 173.34 (11) | C15—C14—H14 | 120.6 |
O3i—Cu1—N2 | 96.69 (11) | C13—C14—H14 | 120.6 |
N1—Cu1—N2 | 80.88 (11) | C14—C15—C16 | 119.8 (4) |
O1—Cu1—C8i | 82.87 (11) | C14—C15—H15 | 120.1 |
O3i—Cu1—C8i | 29.60 (11) | C16—C15—H15 | 120.1 |
N2—Cu1—C8i | 103.60 (11) | C17—C16—C15 | 119.0 (4) |
N1—Cu1—C8i | 144.33 (12) | C17—C16—H16 | 120.5 |
C1—O1—Cu1 | 106.8 (2) | C15—C16—H16 | 120.5 |
C8—O3—Cu1ii | 101.3 (2) | N1—C17—C16 | 121.4 (3) |
C17—N1—C13 | 118.9 (3) | N1—C17—C18 | 114.0 (3) |
C17—N1—Cu1 | 115.6 (2) | C16—C17—C18 | 124.6 (3) |
C13—N1—Cu1 | 125.4 (2) | N2—C18—C19 | 121.3 (3) |
C22—N2—C18 | 118.9 (3) | N2—C18—C17 | 114.2 (3) |
C22—N2—Cu1 | 125.8 (2) | C19—C18—C17 | 124.5 (3) |
C18—N2—Cu1 | 115.3 (2) | C20—C19—C18 | 118.7 (4) |
O2—C1—O1 | 123.0 (3) | C20—C19—H19 | 120.7 |
O2—C1—C2 | 120.3 (3) | C18—C19—H19 | 120.7 |
O1—C1—C2 | 116.7 (3) | C19—C20—C21 | 120.0 (4) |
C3—C2—C7 | 120.3 (3) | C19—C20—H20 | 120.0 |
C3—C2—C1 | 120.6 (3) | C21—C20—H20 | 120.0 |
C7—C2—C1 | 119.1 (3) | C22—C21—C20 | 118.2 (4) |
C2—C3—C4 | 119.3 (3) | C22—C21—H21 | 120.9 |
C2—C3—H3 | 120.4 | C20—C21—H21 | 120.9 |
C4—C3—H3 | 120.4 | N2—C22—C21 | 123.0 (4) |
C5—C4—C3 | 119.4 (3) | N2—C22—H22 | 118.5 |
C5—C4—C8 | 119.7 (3) | C21—C22—H22 | 118.5 |
C3—C4—C8 | 120.9 (3) | ||
O3i—Cu1—O1—C1 | 84.9 (3) | C3—C4—C8—Cu1ii | 47.6 (8) |
N1—Cu1—O1—C1 | −101.7 (3) | C5—C6—C9—C12 | −6.0 (7) |
C8i—Cu1—O1—C1 | 114.1 (3) | C7—C6—C9—C12 | 174.1 (5) |
O1—Cu1—N1—C17 | 176.4 (2) | C5—C6—C9—C12' | 32.7 (7) |
N2—Cu1—N1—C17 | 1.5 (2) | C7—C6—C9—C12' | −147.2 (5) |
C8i—Cu1—N1—C17 | −99.1 (3) | C5—C6—C9—C10' | 169.2 (6) |
N2—Cu1—N1—C13 | −180.0 (3) | C7—C6—C9—C10' | −10.7 (8) |
C8i—Cu1—N1—C13 | 79.4 (3) | C5—C6—C9—C11 | −126.8 (5) |
O3i—Cu1—N2—C22 | −7.2 (3) | C7—C6—C9—C11 | 53.3 (7) |
N1—Cu1—N2—C22 | 179.6 (3) | C5—C6—C9—C10 | 116.6 (5) |
C8i—Cu1—N2—C22 | −36.5 (3) | C7—C6—C9—C10 | −63.3 (6) |
O3i—Cu1—N2—C18 | 172.5 (2) | C5—C6—C9—C11' | −77.6 (6) |
N1—Cu1—N2—C18 | −0.6 (2) | C7—C6—C9—C11' | 102.6 (5) |
C8i—Cu1—N2—C18 | 143.3 (2) | C17—N1—C13—C14 | 1.8 (5) |
Cu1—O1—C1—O2 | 17.2 (5) | Cu1—N1—C13—C14 | −176.7 (3) |
Cu1—O1—C1—C2 | −162.2 (3) | N1—C13—C14—C15 | −1.4 (6) |
O2—C1—C2—C3 | 18.7 (6) | C13—C14—C15—C16 | −0.1 (6) |
O1—C1—C2—C3 | −162.0 (3) | C14—C15—C16—C17 | 1.1 (6) |
O2—C1—C2—C7 | −160.4 (4) | C13—N1—C17—C16 | −0.7 (5) |
O1—C1—C2—C7 | 19.0 (5) | Cu1—N1—C17—C16 | 178.0 (3) |
C7—C2—C3—C4 | −0.7 (5) | C13—N1—C17—C18 | 179.3 (3) |
C1—C2—C3—C4 | −179.7 (3) | Cu1—N1—C17—C18 | −2.1 (4) |
C2—C3—C4—C5 | 1.7 (5) | C15—C16—C17—N1 | −0.7 (6) |
C2—C3—C4—C8 | −178.1 (3) | C15—C16—C17—C18 | 179.3 (3) |
C3—C4—C5—C6 | −0.5 (5) | C22—N2—C18—C19 | −0.1 (5) |
C8—C4—C5—C6 | 179.3 (3) | Cu1—N2—C18—C19 | −179.8 (3) |
C4—C5—C6—C7 | −1.7 (6) | C22—N2—C18—C17 | 179.5 (3) |
C4—C5—C6—C9 | 178.4 (4) | Cu1—N2—C18—C17 | −0.3 (4) |
C3—C2—C7—C6 | −1.7 (6) | N1—C17—C18—N2 | 1.5 (4) |
C1—C2—C7—C6 | 177.4 (4) | C16—C17—C18—N2 | −178.5 (3) |
C5—C6—C7—C2 | 2.8 (6) | N1—C17—C18—C19 | −178.9 (3) |
C9—C6—C7—C2 | −177.3 (4) | C16—C17—C18—C19 | 1.1 (5) |
Cu1ii—O3—C8—O4 | −22.7 (4) | N2—C18—C19—C20 | 0.4 (5) |
Cu1ii—O3—C8—C4 | 155.6 (2) | C17—C18—C19—C20 | −179.2 (3) |
C5—C4—C8—O4 | −3.7 (5) | C18—C19—C20—C21 | −0.8 (6) |
C3—C4—C8—O4 | 176.1 (3) | C19—C20—C21—C22 | 0.9 (6) |
C5—C4—C8—O3 | 178.0 (3) | C18—N2—C22—C21 | 0.2 (5) |
C3—C4—C8—O3 | −2.2 (5) | Cu1—N2—C22—C21 | 180.0 (3) |
C5—C4—C8—Cu1ii | −132.2 (6) | C20—C21—C22—N2 | −0.6 (6) |