| Bruker SMART APEXII CCD area-detector diffractometer | 7380 independent reflections |
| Radiation source: fine-focus sealed tube | 6571 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.020 |
| T = 100.0(1) K | θmax = 37.5º |
| φ and ω scans | θmin = 2.6º |
| Absorption correction: multi-scan(SADABS; Bruker, 2005) | h = −11→11 |
| Tmin = 0.932, Tmax = 0.976 | k = −11→10 |
| 31311 measured reflections | l = −27→27 |