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. 2008 Nov 29;64(Pt 12):o2469. doi: 10.1107/S160053680803941X
Rigaku Saturn diffractometer 4492 independent reflections
Radiation source: rotating anode 3911 reflections with I > 2σ(I)
Monochromator: confocal Rint = 0.039
Detector resolution: 7.31 pixels mm-1 θmax = 27.9º
T = 113(2) K θmin = 2.5º
ω scans h = −11→11
Absorption correction: multi-scan(CrystalClear; Rigaku/MSC, 2002) k = −34→35
Tmin = 0.961, Tmax = 0.968 l = −11→11
18499 measured reflections