| Rigaku Saturn diffractometer | 4492 independent reflections |
| Radiation source: rotating anode | 3911 reflections with I > 2σ(I) |
| Monochromator: confocal | Rint = 0.039 |
| Detector resolution: 7.31 pixels mm-1 | θmax = 27.9º |
| T = 113(2) K | θmin = 2.5º |
| ω scans | h = −11→11 |
| Absorption correction: multi-scan(CrystalClear; Rigaku/MSC, 2002) | k = −34→35 |
| Tmin = 0.961, Tmax = 0.968 | l = −11→11 |
| 18499 measured reflections |