Bruker SMART APEXII CCD diffractometer | 8005 independent reflections |
Radiation source: fine-focus sealed tube | 6952 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.031 |
T = 100(2) K | θmax = 28.0º |
φ and ω scans | θmin = 1.5º |
Absorption correction: multi-scan(SADABS; Bruker, 2005) | h = −14→14 |
Tmin = 0.204, Tmax = 0.346 | k = −16→16 |
22723 measured reflections | l = −18→18 |