Table 2. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| N1—H1B⋯O2 | 0.82 (5) | 2.21 (9) | 2.879 (7) | 139 (11) |
| N1—H1A⋯O9i | 0.90 (5) | 2.08 (5) | 2.976 (8) | 174 (10) |
| N2—H2B⋯O4 | 0.82 (4) | 2.21 (7) | 2.870 (7) | 139 (10) |
| N2—H2A⋯O11ii | 0.89 (4) | 2.56 (8) | 3.235 (8) | 134 (9) |
| N2—H2A⋯O12ii | 0.89 (4) | 2.05 (5) | 2.916 (8) | 164 (10) |
| N3—H3A⋯O5 | 0.88 (5) | 2.12 (5) | 2.991 (7) | 175 (11) |
| N3—H3B⋯O7 | 0.86 (5) | 2.18 (8) | 2.900 (7) | 141 (10) |
| N4—H4A⋯O1iii | 0.81 (5) | 2.51 (9) | 3.148 (8) | 136 (10) |
| N4—H4A⋯O3iii | 0.81 (5) | 2.26 (6) | 3.027 (8) | 159 (11) |
| N4—H4B⋯O10 | 0.85 (5) | 2.13 (8) | 2.877 (8) | 146 (11) |
Symmetry codes: (i)
; (ii)
; (iii)
.