| Refinement on F2 | Hydrogen site location: inferred from neighbouring sites |
| Least-squares matrix: full | H-atom parameters constrained |
| R[F2 > 2σ(F2)] = 0.043 | w = 1/[σ2(Fo2) + (0.0709P)2 + 0.0494P] where P = (Fo2 + 2Fc2)/3 |
| wR(F2) = 0.111 | (Δ/σ)max = 0.001 |
| S = 1.04 | Δρmax = 0.24 e Å−3 |
| 4350 reflections | Δρmin = −0.16 e Å−3 |
| 238 parameters | Extinction correction: none |
| Primary atom site location: structure-invariant direct methods | Absolute structure: Flack (1983); 1846 Friedel pairs |
| Secondary atom site location: difference Fourier map | Flack parameter: 0.65 (6) |