| Stoe IPDS diffractometer | 3982 independent reflections |
| Radiation source: fine-focus sealed tube | 3026 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.079 |
| T = 183(2) K | θmax = 25.0º |
| φ oscillation scan | θmin = 2.8º |
| Absorption correction: numerical(Coppens et al., 1965) | h = −15→15 |
| Tmin = 0.329, Tmax = 0.499 | k = −20→20 |
| 52250 measured reflections | l = −24→24 |
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