Bruker SMART APEX CCD diffractometer | 3114 independent reflections |
Radiation source: fine-focus sealed tube | 2553 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.055 |
T = 298(2) K | θmax = 28.3º |
φ and ω scans | θmin = 2.1º |
Absorption correction: multi-scan(SADABS; Bruker, 2002) | h = −10→9 |
Tmin = 0.379, Tmax = 0.469 | k = −10→7 |
4603 measured reflections | l = −13→12 |