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. 2008 Jan 4;64(Pt 2):m287–m288. doi: 10.1107/S1600536807067979
Bruker SMART APEX CCD diffractometer 3114 independent reflections
Radiation source: fine-focus sealed tube 2553 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.055
T = 298(2) K θmax = 28.3º
φ and ω scans θmin = 2.1º
Absorption correction: multi-scan(SADABS; Bruker, 2002) h = −10→9
Tmin = 0.379, Tmax = 0.469 k = −10→7
4603 measured reflections l = −13→12