| STOE IPDS-II diffractometer | 1325 independent reflections |
| Radiation source: fine-focus sealed tube | 991 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.068 |
| Detector resolution: 6.67 pixels mm-1 | θmax = 26.0º |
| T = 296(2) K | θmin = 2.6º |
| rotation method scans | h = −10→10 |
| Absorption correction: integration(X-RED32; Stoe & Cie, 2002) | k = −11→11 |
| Tmin = 0.765, Tmax = 0.916 | l = −12→12 |
| 5532 measured reflections |
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