| Bruker KAPPA APEXII CCD diffractometer | 3012 independent reflections |
| Radiation source: fine-focus sealed tube | 1817 reflections with I > 3σ(I) |
| Monochromator: graphite | Rint = 0.032 |
| Detector resolution: 8.33 pixels mm-1 | θmax = 28.3º |
| T = 296(2) K | θmin = 2.0º |
| ω scans | h = −10→10 |
| Absorption correction: multi-scan(SADABS; Bruker, 2005) | k = −11→11 |
| Tmin = 0.935, Tmax = 0.958 | l = −14→14 |
| 11895 measured reflections |