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. 2008 Jan 9;64(Pt 2):o389. doi: 10.1107/S160053680800007X
Bruker KAPPA APEXII CCD diffractometer 3012 independent reflections
Radiation source: fine-focus sealed tube 1817 reflections with I > 3σ(I)
Monochromator: graphite Rint = 0.032
Detector resolution: 8.33 pixels mm-1 θmax = 28.3º
T = 296(2) K θmin = 2.0º
ω scans h = −10→10
Absorption correction: multi-scan(SADABS; Bruker, 2005) k = −11→11
Tmin = 0.935, Tmax = 0.958 l = −14→14
11895 measured reflections