Rigaku R-AXIS Spider diffractometer	5171 independent reflections
Radiation source: fine-focus sealed tube	3376 reflections with I > 2σ(I)
Monochromator: graphite	Rint = 0.024
T = 153(2) K	θmax = 27.5º
ω scans	θmin = 3.1º
Absorption correction: empirical (using intensity measurements)(ABSCOR; Higashi, 1995)	h = −10→10
Tmin = 0.919, Tmax = 0.966	k = −12→12
11326 measured reflections	l = −18→18