| Br10—C11 | 1.902 (7) | C31—H31B | 0.9800 |
| C10—C11 | 1.375 (9) | C31—H31C | 0.9800 |
| C10—O10 | 1.379 (8) | O10—C40 | 1.408 (15) |
| C10—C15 | 1.394 (9) | O10—C41 | 1.511 (14) |
| C11—C12 | 1.379 (10) | C40—H40A | 0.9800 |
| C12—C13 | 1.388 (10) | C40—H40B | 0.9800 |
| C12—H12 | 0.9500 | C40—H40C | 0.9800 |
| C13—C14 | 1.398 (9) | C41—H41A | 0.9800 |
| C13—C16 | 1.539 (10) | C41—H41B | 0.9800 |
| C14—C15 | 1.397 (9) | C41—H41C | 0.9800 |
| C14—H14 | 0.9500 | C50—H50A | 0.9800 |
| C15—C20 | 1.493 (9) | C50—H50B | 0.9800 |
| C16—C71 | 1.499 (11) | C50—H50C | 0.9800 |
| C16—C70 | 1.507 (13) | C51—H51A | 0.9800 |
| C16—C72 | 1.510 (11) | C51—H51B | 0.9800 |
| Br21—C22 | 1.899 (6) | C51—H51C | 0.9800 |
| C20—C21 | 1.390 (9) | C52—H52A | 0.9800 |
| C20—C25 | 1.401 (9) | C52—H52B | 0.9800 |
| C21—O21 | 1.380 (7) | C52—H52C | 0.9800 |
| C21—C22 | 1.388 (9) | C60—H60A | 0.9800 |
| C22—C23 | 1.380 (9) | C60—H60B | 0.9800 |
| C23—C24 | 1.398 (9) | C60—H60C | 0.9800 |
| C23—H23 | 0.9500 | C61—H61A | 0.9800 |
| C24—C25 | 1.385 (8) | C61—H61B | 0.9800 |
| C24—C26 | 1.541 (9) | C61—H61C | 0.9800 |
| C25—H25 | 0.9500 | C62—H62A | 0.9800 |
| C26—C60 | 1.489 (15) | C62—H62B | 0.9800 |
| C26—C52 | 1.519 (17) | C62—H62C | 0.9800 |
| C26—C61 | 1.533 (15) | C70—H70A | 0.9800 |
| C26—C51 | 1.550 (17) | C70—H70B | 0.9800 |
| C26—C50 | 1.555 (15) | C70—H70C | 0.9800 |
| C26—C62 | 1.563 (15) | C71—H71A | 0.9800 |
| O21—C30 | 1.516 (14) | C71—H71B | 0.9800 |
| O21—C31 | 1.530 (15) | C71—H71C | 0.9800 |
| C30—H30A | 0.9800 | C72—H72A | 0.9800 |
| C30—H30B | 0.9800 | C72—H72B | 0.9800 |
| C30—H30C | 0.9800 | C72—H72C | 0.9800 |
| C31—H31A | 0.9800 | ||
| C11—C10—O10 | 121.0 (6) | O21—C30—H30A | 109.5 |
| C11—C10—C15 | 119.0 (7) | O21—C30—H30B | 109.5 |
| O10—C10—C15 | 120.0 (6) | O21—C30—H30C | 109.5 |
| C10—C11—C12 | 121.3 (7) | O21—C31—H31A | 109.5 |
| C10—C11—Br10 | 119.5 (6) | O21—C31—H31B | 109.5 |
| C12—C11—Br10 | 119.2 (5) | H31A—C31—H31B | 109.5 |
| C11—C12—C13 | 121.6 (6) | O21—C31—H31C | 109.5 |
| C11—C12—H12 | 119.2 | H31A—C31—H31C | 109.5 |
| C13—C12—H12 | 119.2 | H31B—C31—H31C | 109.5 |
| C12—C13—C14 | 116.8 (6) | C10—O10—C40 | 110.5 (8) |
| C12—C13—C16 | 122.8 (6) | C10—O10—C41 | 117.3 (7) |
| C14—C13—C16 | 120.5 (6) | C40—O10—C41 | 131.4 (9) |
| C15—C14—C13 | 122.1 (6) | O10—C40—H40A | 109.5 |
| C15—C14—H14 | 118.9 | O10—C40—H40B | 109.5 |
| C13—C14—H14 | 118.9 | H40A—C40—H40B | 109.5 |
| C10—C15—C14 | 119.2 (6) | O10—C40—H40C | 109.5 |
| C10—C15—C20 | 119.8 (6) | H40A—C40—H40C | 109.5 |
| C14—C15—C20 | 121.1 (6) | H40B—C40—H40C | 109.5 |
| C71—C16—C70 | 105.5 (8) | O10—C41—H41A | 109.5 |
| C71—C16—C72 | 109.2 (7) | O10—C41—H41B | 109.5 |
| C70—C16—C72 | 110.6 (8) | O10—C41—H41C | 109.5 |
| C71—C16—C13 | 113.3 (7) | C26—C50—H50A | 109.5 |
| C70—C16—C13 | 108.3 (7) | C26—C50—H50B | 109.5 |
| C72—C16—C13 | 110.0 (6) | C26—C50—H50C | 109.5 |
| C21—C20—C25 | 119.0 (6) | C26—C51—H51A | 109.5 |
| C21—C20—C15 | 120.6 (6) | C26—C51—H51B | 109.5 |
| C25—C20—C15 | 120.4 (6) | C26—C51—H51C | 109.5 |
| O21—C21—C22 | 121.0 (5) | C26—C52—H52A | 109.5 |
| O21—C21—C20 | 120.0 (6) | C26—C52—H52B | 109.5 |
| C22—C21—C20 | 119.0 (6) | C26—C52—H52C | 109.5 |
| C23—C22—C21 | 121.5 (6) | C26—C60—H60A | 109.5 |
| C23—C22—Br21 | 119.5 (5) | C26—C60—H60B | 109.5 |
| C21—C22—Br21 | 119.0 (5) | H60A—C60—H60B | 109.5 |
| C22—C23—C24 | 120.4 (6) | C26—C60—H60C | 109.5 |
| C22—C23—H23 | 119.8 | H60A—C60—H60C | 109.5 |
| C24—C23—H23 | 119.8 | H60B—C60—H60C | 109.5 |
| C25—C24—C23 | 117.8 (6) | C26—C61—H61A | 109.5 |
| C25—C24—C26 | 121.5 (5) | C26—C61—H61B | 109.5 |
| C23—C24—C26 | 120.7 (5) | H61A—C61—H61B | 109.5 |
| C24—C25—C20 | 122.2 (6) | C26—C61—H61C | 109.5 |
| C24—C25—H25 | 118.9 | H61A—C61—H61C | 109.5 |
| C20—C25—H25 | 118.9 | H61B—C61—H61C | 109.5 |
| C60—C26—C52 | 140.6 (10) | C26—C62—H62A | 109.5 |
| C60—C26—C61 | 112.2 (10) | C26—C62—H62B | 109.5 |
| C52—C26—C61 | 47.7 (9) | H62A—C62—H62B | 109.5 |
| C60—C26—C24 | 108.2 (8) | C26—C62—H62C | 109.5 |
| C52—C26—C24 | 110.8 (8) | H62A—C62—H62C | 109.5 |
| C61—C26—C24 | 110.4 (7) | H62B—C62—H62C | 109.5 |
| C60—C26—C51 | 49.9 (9) | C16—C70—H70A | 109.5 |
| C52—C26—C51 | 110.2 (11) | C16—C70—H70B | 109.5 |
| C61—C26—C51 | 65.6 (10) | H70A—C70—H70B | 109.5 |
| C24—C26—C51 | 109.0 (8) | C16—C70—H70C | 109.5 |
| C60—C26—C50 | 60.0 (9) | H70A—C70—H70C | 109.5 |
| C52—C26—C50 | 107.0 (10) | H70B—C70—H70C | 109.5 |
| C61—C26—C50 | 134.6 (9) | C16—C71—H71A | 109.5 |
| C24—C26—C50 | 114.4 (7) | C16—C71—H71B | 109.5 |
| C51—C26—C50 | 105.3 (10) | H71A—C71—H71B | 109.5 |
| C60—C26—C62 | 111.6 (9) | C16—C71—H71C | 109.5 |
| C52—C26—C62 | 61.4 (9) | H71A—C71—H71C | 109.5 |
| C61—C26—C62 | 107.3 (9) | H71B—C71—H71C | 109.5 |
| C24—C26—C62 | 107.1 (7) | C16—C72—H72A | 109.5 |
| C51—C26—C62 | 143.3 (9) | C16—C72—H72B | 109.5 |
| C50—C26—C62 | 52.4 (8) | H72A—C72—H72B | 109.5 |
| C21—O21—C30 | 111.6 (7) | C16—C72—H72C | 109.5 |
| C21—O21—C31 | 111.4 (7) | H72A—C72—H72C | 109.5 |
| C30—O21—C31 | 136.5 (8) | H72B—C72—H72C | 109.5 |