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. 2008 Jan 4;64(Pt 2):o358. doi: 10.1107/S1600536807067888
MacScience DIPLabo 32001 diffractometer 3818 independent reflections
Radiation source: fine-focus sealed tube 2917 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.024
Detector resolution: 10.0 pixels mm-1 θmax = 25.0º
T = 295(2) K θmin = 2.3º
ω scans h = −11→11
Absorption correction: none k = −15→15
7255 measured reflections l = −22→22