Oxford Xcalibur3 CCD area-detector diffractometer	1578 independent reflections
Radiation source: fine-focus sealed tube	956 reflections with I > 2σ(I)
Monochromator: graphite	Rint = 0.040
Detector resolution: 15.9809 pixels mm-1	θmax = 26.0º
T = 200(2) K	θmin = 4.3º
ω scans	h = −15→9
Absorption correction: multi-scan(CrysAlis RED; Oxford Diffraction, 2007)	k = −19→31
Tmin = 0.899, Tmax = 0.990	l = −5→6
5871 measured reflections