Bruker APEXII CCD diffractometer | 1948 independent reflections |
Radiation source: fine-focus sealed tube | 1887 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.015 |
T = 298(2) K | θmax = 25.0º |
ω scans | θmin = 2.7º |
Absorption correction: multi-scan(SADABS; Sheldrick, 2003) | h = −8→9 |
Tmin = 0.956, Tmax = 0.993 | k = −6→6 |
3073 measured reflections | l = −17→17 |