| Bruker SMART APEX2 CCD area-detector diffractometer | 2664 independent reflections |
| Radiation source: fine-focus sealed tube | 2575 reflections with I > 2/s(I) |
| Monochromator: graphite | Rint = 0.035 |
| Detector resolution: 0 pixels mm-1 | θmax = 29.0º |
| T = 100(2) K | θmin = 2.7º |
| φ and ω scans | h = −10→10 |
| Absorption correction: multi-scan(APEX2; Bruker, 2005) | k = −25→25 |
| Tmin = 0.386, Tmax = 0.455 | l = −9→9 |
| 10713 measured reflections |
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