| Bruker SMART CCD area-detector diffractometer | 1641 independent reflections |
| Radiation source: fine-focus sealed tube | 1457 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.011 |
| T = 295(2) K | θmax = 25.5º |
| φ and ω scans | θmin = 2.8º |
| Absorption correction: multi-scan(SADABS; Bruker, 2002) | h = −5→5 |
| Tmin = 0.765, Tmax = 0.872 | k = −9→9 |
| 2415 measured reflections | l = −15→15 |
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