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. 2008 Jan 18;64(Pt 2):o471. doi: 10.1107/S160053680800130X
Bruker SMART APEX area-detector diffractometer 3094 independent reflections
Radiation source: fine-focus sealed tube 2579 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.021
T = 298(2) K θmax = 27.0º
ω scans θmin = 2.6º
Absorption correction: multi-scan(SADABS; Sheldrick, 1996) h = −16→17
Tmin = 0.975, Tmax = 0.976 k = −12→12
11531 measured reflections l = −14→14