Bruker SMART APEX area-detector diffractometer | 3094 independent reflections |
Radiation source: fine-focus sealed tube | 2579 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.021 |
T = 298(2) K | θmax = 27.0º |
ω scans | θmin = 2.6º |
Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −16→17 |
Tmin = 0.975, Tmax = 0.976 | k = −12→12 |
11531 measured reflections | l = −14→14 |