Cu1—N1 | 1.966 (4) | N7—H22 | 0.96 (2) |
Cu1—O1 | 1.986 (3) | N7—H23 | 0.95 (2) |
Cu1—N2 | 1.991 (4) | C1—C2 | 1.406 (8) |
Cu1—O2 | 2.000 (3) | C1—H1 | 0.9500 |
Cu1—O3 | 2.252 (4) | C2—C3 | 1.382 (9) |
Cu1—O4 | 2.610 (4) | C2—H2 | 0.9500 |
Cu2—N5 | 1.955 (4) | C3—C4 | 1.362 (8) |
Cu2—O7 | 1.966 (3) | C3—H3 | 0.9500 |
Cu2—O8 | 1.981 (3) | C4—C5 | 1.397 (7) |
Cu2—N6 | 1.994 (4) | C4—H4 | 0.9500 |
Cu2—O9 | 2.337 (3) | C5—C6 | 1.458 (8) |
Cu2—O10 | 2.541 (4) | C6—C7 | 1.514 (7) |
O1—C8 | 1.254 (5) | C7—H7A | 0.9800 |
O2—C8i | 1.258 (5) | C7—H7B | 0.9800 |
O3—H18 | 0.96 (2) | C7—H7C | 0.9800 |
O3—H19 | 0.95 (2) | C8—O2i | 1.258 (5) |
O4—N4 | 1.248 (5) | C8—C8i | 1.527 (9) |
O5—N4 | 1.227 (6) | C9—C10 | 1.386 (7) |
O6—N4 | 1.260 (5) | C9—H9 | 0.9500 |
O7—C16 | 1.262 (5) | C10—C11 | 1.378 (8) |
O8—C16ii | 1.258 (5) | C10—H10 | 0.9500 |
O9—C17 | 1.409 (6) | C11—C12 | 1.384 (8) |
O9—H24 | 0.8400 | C11—H11 | 0.9500 |
O10—N8 | 1.237 (5) | C12—C13 | 1.398 (7) |
O11—N8 | 1.228 (6) | C12—H12 | 0.9500 |
O12—N8 | 1.247 (6) | C13—C14 | 1.457 (7) |
N1—C1 | 1.315 (7) | C14—C15 | 1.508 (7) |
N1—C5 | 1.356 (6) | C15—H15A | 0.9800 |
N2—C6 | 1.273 (7) | C15—H15B | 0.9800 |
N2—N3 | 1.360 (6) | C15—H15C | 0.9800 |
N3—H20 | 0.95 (2) | C16—O8ii | 1.258 (5) |
N3—H21 | 0.97 (2) | C16—C16ii | 1.520 (9) |
N5—C9 | 1.313 (7) | C17—H17A | 0.9800 |
N5—C13 | 1.381 (6) | C17—H17B | 0.9800 |
N6—C14 | 1.277 (6) | C17—H17C | 0.9800 |
N6—N7 | 1.381 (6) | ||
N1—Cu1—O1 | 174.12 (15) | O11—N8—O10 | 120.4 (5) |
N1—Cu1—N2 | 80.65 (18) | O11—N8—O12 | 120.7 (5) |
O1—Cu1—N2 | 95.44 (16) | O10—N8—O12 | 118.9 (5) |
N1—Cu1—O2 | 98.76 (16) | N1—C1—C2 | 121.7 (6) |
O1—Cu1—O2 | 84.01 (13) | N1—C1—H1 | 119.2 |
N2—Cu1—O2 | 166.68 (14) | C2—C1—H1 | 119.2 |
N1—Cu1—O3 | 86.33 (15) | C3—C2—C1 | 117.6 (6) |
O1—Cu1—O3 | 98.48 (13) | C3—C2—H2 | 121.2 |
N2—Cu1—O3 | 95.43 (16) | C1—C2—H2 | 121.2 |
O2—Cu1—O3 | 97.82 (14) | C4—C3—C2 | 120.4 (5) |
N1—Cu1—O4 | 83.01 (14) | C4—C3—H3 | 119.8 |
O1—Cu1—O4 | 91.90 (12) | C2—C3—H3 | 119.8 |
N2—Cu1—O4 | 78.20 (14) | C3—C4—C5 | 119.7 (6) |
O2—Cu1—O4 | 88.50 (12) | C3—C4—H4 | 120.1 |
O3—Cu1—O4 | 168.33 (13) | C5—C4—H4 | 120.1 |
N5—Cu2—O7 | 177.14 (15) | N1—C5—C4 | 119.5 (5) |
N5—Cu2—O8 | 95.30 (15) | N1—C5—C6 | 115.2 (4) |
O7—Cu2—O8 | 85.09 (13) | C4—C5—C6 | 125.3 (5) |
N5—Cu2—N6 | 81.51 (17) | N2—C6—C5 | 114.2 (4) |
O7—Cu2—N6 | 97.92 (15) | N2—C6—C7 | 123.9 (5) |
O8—Cu2—N6 | 175.14 (15) | C5—C6—C7 | 121.8 (5) |
N5—Cu2—O9 | 89.35 (14) | C6—C7—H7A | 109.5 |
O7—Cu2—O9 | 93.43 (13) | C6—C7—H7B | 109.5 |
O8—Cu2—O9 | 95.95 (13) | H7A—C7—H7B | 109.5 |
N6—Cu2—O9 | 87.70 (14) | C6—C7—H7C | 109.5 |
N5—Cu2—O10 | 85.40 (14) | H7A—C7—H7C | 109.5 |
O7—Cu2—O10 | 91.78 (13) | H7B—C7—H7C | 109.5 |
O8—Cu2—O10 | 87.50 (13) | O1—C8—O2i | 126.0 (4) |
N6—Cu2—O10 | 88.58 (14) | O1—C8—C8i | 117.4 (5) |
O9—Cu2—O10 | 173.97 (12) | O2i—C8—C8i | 116.6 (5) |
C8—O1—Cu1 | 111.0 (3) | N5—C9—C10 | 122.3 (5) |
C8i—O2—Cu1 | 110.9 (3) | N5—C9—H9 | 118.9 |
Cu1—O3—H18 | 106 (4) | C10—C9—H9 | 118.9 |
Cu1—O3—H19 | 126 (3) | C11—C10—C9 | 118.0 (5) |
H18—O3—H19 | 92 (5) | C11—C10—H10 | 121.0 |
N4—O4—Cu1 | 110.5 (3) | C9—C10—H10 | 121.0 |
C16—O7—Cu2 | 110.2 (3) | C10—C11—C12 | 120.7 (5) |
C16ii—O8—Cu2 | 110.3 (3) | C10—C11—H11 | 119.7 |
C17—O9—Cu2 | 119.5 (3) | C12—C11—H11 | 119.7 |
C17—O9—H24 | 109.5 | C11—C12—C13 | 119.1 (5) |
Cu2—O9—H24 | 116.3 | C11—C12—H12 | 120.4 |
N8—O10—Cu2 | 113.3 (3) | C13—C12—H12 | 120.4 |
C1—N1—C5 | 121.1 (5) | N5—C13—C12 | 118.7 (5) |
C1—N1—Cu1 | 125.4 (4) | N5—C13—C14 | 115.4 (4) |
C5—N1—Cu1 | 113.4 (3) | C12—C13—C14 | 125.9 (5) |
C6—N2—N3 | 121.3 (5) | N6—C14—C13 | 114.4 (4) |
C6—N2—Cu1 | 116.4 (4) | N6—C14—C15 | 123.1 (5) |
N3—N2—Cu1 | 122.0 (3) | C13—C14—C15 | 122.5 (4) |
N2—N3—H20 | 110 (5) | C14—C15—H15A | 109.5 |
N2—N3—H21 | 108 (5) | C14—C15—H15B | 109.5 |
H20—N3—H21 | 116 (7) | H15A—C15—H15B | 109.5 |
O5—N4—O4 | 120.6 (5) | C14—C15—H15C | 109.5 |
O5—N4—O6 | 120.2 (5) | H15A—C15—H15C | 109.5 |
O4—N4—O6 | 119.2 (4) | H15B—C15—H15C | 109.5 |
C9—N5—C13 | 121.2 (4) | O8ii—C16—O7 | 125.8 (4) |
C9—N5—Cu2 | 126.3 (3) | O8ii—C16—C16ii | 116.7 (5) |
C13—N5—Cu2 | 112.6 (3) | O7—C16—C16ii | 117.6 (5) |
C14—N6—N7 | 121.9 (4) | O9—C17—H17A | 109.5 |
C14—N6—Cu2 | 115.9 (4) | O9—C17—H17B | 109.5 |
N7—N6—Cu2 | 121.5 (3) | H17A—C17—H17B | 109.5 |
N6—N7—H22 | 106 (4) | O9—C17—H17C | 109.5 |
N6—N7—H23 | 111 (4) | H17A—C17—H17C | 109.5 |
H22—N7—H23 | 119 (5) | H17B—C17—H17C | 109.5 |