| Nonius KappaCCD diffractometer | 1699 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.055 |
| Detector resolution: 9 pixels mm-1 | θmax = 27.5º |
| T = 173(2) K | θmin = 2.9º |
| CCD scans | h = −9→9 |
| Absorption correction: none | k = −16→15 |
| 11787 measured reflections | l = −15→16 |
| 2485 independent reflections |
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