| Bruker SMART CCD area-detector diffractometer | 2961 independent reflections |
| Radiation source: fine-focus sealed tube | 1543 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.071 |
| T = 298(2) K | θmax = 27.0º |
| ω scans | θmin = 1.7º |
| Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −9→9 |
| Tmin = 0.916, Tmax = 0.926 | k = −29→30 |
| 11286 measured reflections | l = −10→11 |