| [Tc(CO)6]ClO4 | F000 = 704 |
| Mr = 366.42 | Dx = 2.152 Mg m−3 |
| Monoclinic, C2/c | Mo Kα radiation λ = 0.71073 Å |
| Hall symbol: -C 2yc | Cell parameters from 5446 reflections |
| a = 13.227 (4) Å | θ = 2.0–29.6º |
| b = 6.8002 (18) Å | µ = 1.55 mm−1 |
| c = 13.616 (3) Å | T = 293 (2) K |
| β = 112.56 (2)º | Prism, colorless |
| V = 1131.0 (5) Å3 | 0.20 × 0.18 × 0.10 mm |
| Z = 4 |