| Bruker SMART CCD area-detector diffractometer | 7167 independent reflections |
| Radiation source: fine-focus sealed tube | 4463 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.066 |
| T = 298(2) K | θmax = 29.3º |
| φ and ω scans | θmin = 2.2º |
| Absorption correction: multi-scan(SADABS; Sheldrick, 1998) | h = −22→13 |
| Tmin = 0.612, Tmax = 0.860 | k = −13→15 |
| 14309 measured reflections | l = −20→20 |