Rigaku Saturn diffractometer | 6016 independent reflections |
Radiation source: rotating anode | 5436 reflections with I > 2σ(I) |
Monochromator: confocal | Rint = 0.040 |
Detector resolution: 14.63 pixels mm-1 | θmax = 27.9º |
T = 113(2) K | θmin = 1.7º |
ω scans | h = −15→15 |
Absorption correction: multi-scan(CrystalClear; Rigaku, 1999) | k = −14→14 |
Tmin = 0.943, Tmax = 0.967 | l = −25→25 |
30908 measured reflections |