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. 2008 Aug 16;64(Pt 9):o1772–o1773. doi: 10.1107/S1600536808025695
Rigaku Saturn diffractometer 6016 independent reflections
Radiation source: rotating anode 5436 reflections with I > 2σ(I)
Monochromator: confocal Rint = 0.040
Detector resolution: 14.63 pixels mm-1 θmax = 27.9º
T = 113(2) K θmin = 1.7º
ω scans h = −15→15
Absorption correction: multi-scan(CrystalClear; Rigaku, 1999) k = −14→14
Tmin = 0.943, Tmax = 0.967 l = −25→25
30908 measured reflections