Refinement on F2	Secondary atom site location: difference Fourier map
Least-squares matrix: full	Hydrogen site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.055	H-atom parameters constrained
wR(F2) = 0.137	w = 1/[σ2(Fo2) + (0.0579P)2 + 1.0431P] where P = (Fo2 + 2Fc2)/3
S = 1.10	(Δ/σ)max = 0.001
6016 reflections	Δρmax = 0.42 e Å−3
312 parameters	Δρmin = −0.45 e Å−3
112 constraints	Extinction correction: SHELXL97 (Sheldrick, 2008), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4
Primary atom site location: structure-invariant direct methods	Extinction coefficient: 0.0058 (9)