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. 2008 Aug 6;64(Pt 9):o1695. doi: 10.1107/S160053680802521X
Bruker APEXII CCD area-detector diffractometer 1647 independent reflections
Radiation source: fine-focus sealed tube 1229 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.055
T = 298(2) K θmax = 27.0º
ω scans θmin = 1.9º
Absorption correction: multi-scan(SADABS; Sheldrick, 2004) h = −6→6
Tmin = 0.973, Tmax = 0.975 k = −17→16
6081 measured reflections l = −13→13