Bruker APEXII CCD area-detector diffractometer | 1647 independent reflections |
Radiation source: fine-focus sealed tube | 1229 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.055 |
T = 298(2) K | θmax = 27.0º |
ω scans | θmin = 1.9º |
Absorption correction: multi-scan(SADABS; Sheldrick, 2004) | h = −6→6 |
Tmin = 0.973, Tmax = 0.975 | k = −17→16 |
6081 measured reflections | l = −13→13 |