| Bruker SMART CCD area-detector diffractometer | 1689 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.023 |
| Monochromator: graphite | θmax = 25.0º |
| T = 293(2) K | θmin = 1.7º |
| φ and ω scans | h = −7→8 |
| Absorption correction: none | k = −5→9 |
| 3364 measured reflections | l = −14→14 |
| 2229 independent reflections |
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