Nonius KappaCCD diffractometer | 1554 reflections with I > 2σ(I) |
Radiation source: fine-focus sealed tube | Rint = 0.029 |
Monochromator: graphite | θmax = 26.4º |
T = 293(2) K | θmin = 2.1º |
φ and ω scans | h = 0→13 |
Absorption correction: none | k = −7→0 |
14030 measured reflections | l = −25→22 |
2298 independent reflections |