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. 2008 Feb 15;64(Pt 3):o597. doi: 10.1107/S1600536808004169
Nonius KappaCCD diffractometer 1554 reflections with I > 2σ(I)
Radiation source: fine-focus sealed tube Rint = 0.029
Monochromator: graphite θmax = 26.4º
T = 293(2) K θmin = 2.1º
φ and ω scans h = 0→13
Absorption correction: none k = −7→0
14030 measured reflections l = −25→22
2298 independent reflections