| Rigaku R-AXIS RAPID diffractometer | 2917 independent reflections |
| Radiation source: rotating anode | 2652 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.049 |
| Detector resolution: 10.00 pixels mm-1 | θmax = 68.2º |
| T = 296 K | θmin = 4.3º |
| ω scans | h = −9→9 |
| Absorption correction: numerical(NUMABS; Higashi, 1999) | k = −24→24 |
| Tmin = 0.458, Tmax = 0.801 | l = −11→11 |
| 30087 measured reflections |
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