| Nicolet P3 diffractometer | Rint = 0.022 |
| Radiation source: fine-focus sealed tube | θmax = 27.0º |
| Monochromator: graphite | θmin = 2.3º |
| T = 294(2) K | h = 0→5 |
| Wyckoff scan | k = 0→22 |
| Absorption correction: none | l = −13→13 |
| 1004 measured reflections | 3 standard reflections |
| 529 independent reflections | every 50 reflections |
| 437 reflections with I > 2σ(I) | intensity decay: 2% |
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