Bruker SMART CCD diffractometer | 1948 independent reflections |
Radiation source: fine-focus sealed tube | 1391 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.061 |
T = 150(2) K | θmax = 25.3º |
ω scans | θmin = 2.6º |
Absorption correction: multi-scan(SADABS; Bruker, 2004) | h = −14→14 |
Tmin = 0.956, Tmax = 0.972 | k = −14→13 |
10402 measured reflections | l = −18→15 |