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. 2008 Feb 6;64(Pt 3):o556. doi: 10.1107/S1600536808003401
Bruker SMART CCD diffractometer 1948 independent reflections
Radiation source: fine-focus sealed tube 1391 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.061
T = 150(2) K θmax = 25.3º
ω scans θmin = 2.6º
Absorption correction: multi-scan(SADABS; Bruker, 2004) h = −14→14
Tmin = 0.956, Tmax = 0.972 k = −14→13
10402 measured reflections l = −18→15