| Stoe IPDS II diffractometer | 944 independent reflections |
| Monochromator: plane graphite | 720 reflections with I > 2σ(I) |
| Detector resolution: 6.67 pixels mm-1 | Rint = 0.067 |
| T = 296 K | θmax = 26.0º |
| w–scan rotation method | θmin = 2.5º |
| Absorption correction: integration(X-RED32; Stoe & Cie, 2002) | h = −8→8 |
| Tmin = 0.964, Tmax = 0.982 | k = −10→9 |
| 4205 measured reflections | l = −18→18 |
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