Bruker–Nonius KappaCCD diffractometer	4580 independent reflections
Radiation source: fine-focus sealed tube	3182 reflections with I > 2σ(I)
Monochromator: graphite	Rint = 0.054
Detector resolution: 9 pixels mm-1	θmax = 27.5º
T = 150(2) K	θmin = 2.6º
φ scans and ω scans with κ offsets	h = −11→10
Absorption correction: multi-scan(SORTAV; Blessing, 1995)	k = −11→11
Tmin = 0.808, Tmax = 0.980	l = −18→18
10107 measured reflections