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. 2008 Mar 5;64(Pt 4):o668. doi: 10.1107/S1600536808005813
Refinement on F2 Secondary atom site location: difference Fourier map
Least-squares matrix: full Hydrogen site location: inferred from neighbouring sites
R[F2 > 2σ(F2)] = 0.057 H atoms treated by a mixture of independent and constrained refinement
wR(F2) = 0.172   w = 1/[σ2(Fo2) + (0.07P)2] where P = (Fo2 + 2Fc2)/3
S = 0.95 (Δ/σ)max < 0.001
3351 reflections Δρmax = 0.17 e Å3
224 parameters Δρmin = −0.17 e Å3
1 restraint Extinction correction: SHELXTL (Sheldrick, 2008), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4
Primary atom site location: structure-invariant direct methods Extinction coefficient: 0.0051 (12)