| Bruker Kappa APEX2 diffractometer | 3606 independent reflections |
| Radiation source: fine-focus sealed tube | 2160 reflections with I > 2s(I) |
| Monochromator: graphite | Rint = 0.041 |
| T = 295(2) K | θmax = 28.6º |
| ω and φ scan | θmin = 1.8º |
| Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −15→15 |
| Tmin = 0.566, Tmax = 0.620 | k = −10→11 |
| 16472 measured reflections | l = −12→20 |