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. 2008 Mar 29;64(Pt 4):o751. doi: 10.1107/S1600536808007794
Bruker Kappa APEX2 diffractometer 3606 independent reflections
Radiation source: fine-focus sealed tube 2160 reflections with I > 2s(I)
Monochromator: graphite Rint = 0.041
T = 295(2) K θmax = 28.6º
ω and φ scan θmin = 1.8º
Absorption correction: multi-scan(SADABS; Sheldrick, 1996) h = −15→15
Tmin = 0.566, Tmax = 0.620 k = −10→11
16472 measured reflections l = −12→20