| Bruker APEXII CCD diffractometer | 3520 independent reflections |
| Radiation source: sealed tube | 2761 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.031 |
| T = 150(2) K | θmax = 28.9º |
| φ and ω scans | θmin = 2.2º |
| Absorption correction: multi-scan(SADABS; Bruker, 2005) | h = −20→19 |
| Tmin = 0.970, Tmax = 0.991 | k = −6→6 |
| 13445 measured reflections | l = −49→49 |