| Bruker SMART APEX CCD diffractometer | 2164 independent reflections |
| Radiation source: sealed tube | 1840 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.045 |
| T = 213(2) K | θmax = 25.4º |
| φ and ω scans | θmin = 3.0º |
| Absorption correction: multi-scan(SADABS; Bruker, 2000) | h = −10→10 |
| Tmin = 0.642, Tmax = 0.719 | k = −7→8 |
| 11059 measured reflections | l = −22→22 |