| Stoe IPDSII diffractometer | 3613 independent reflections |
| Radiation source: fine-focus sealed tube | 2409 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.061 |
| T = 296(2) K | θmax = 26.0º |
| ω scans | θmin = 2.6º |
| Absorption correction: integration(X-RED32; Stoe & Cie, 2002) | h = −10→10 |
| Tmin = 0.636, Tmax = 0.862 | k = −16→13 |
| 17799 measured reflections | l = −38→38 |
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