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. 2008 Mar 29;64(Pt 4):o749. doi: 10.1107/S1600536808007678
Bruker Kappa APEXII diffractometer 2770 independent reflections
Radiation source: fine-focus sealed tube 1822 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.045
T = 295(2) K θmax = 25.0º
ω and φ scans θmin = 2.2º
Absorption correction: multi-scan(SADABS; Sheldrick, 1996) h = −14→13
Tmin = 0.559, Tmax = 0.665 k = −19→19
14367 measured reflections l = −10→10