Bruker Kappa APEXII diffractometer | 2770 independent reflections |
Radiation source: fine-focus sealed tube | 1822 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.045 |
T = 295(2) K | θmax = 25.0º |
ω and φ scans | θmin = 2.2º |
Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −14→13 |
Tmin = 0.559, Tmax = 0.665 | k = −19→19 |
14367 measured reflections | l = −10→10 |