Oxford Xcalibur diffractometer |
2087 independent reflections |
Radiation source: fine-focus sealed tube |
1773 reflections with I > 2σ(I) |
Monochromator: graphite |
Rint = 0.026 |
Detector resolution: 10.434 pixels mm-1
|
θmax = 25.8º |
T = 295(2) K |
θmin = 5.6º |
φ scans, and ω scans with κ offsets |
h = −6→6 |
Absorption correction: analytical[CrysAlis RED (Oxford Diffraction, 2007). Analytical absorption
correction
using a multifaceted crystal model based on expressions derived
by Clark & Reid (1995)] |
k = −9→9 |
Tmin = 0.852, Tmax = 0.975 |
l = −16→16 |
23656 measured reflections |
|