| Oxford Xcalibur diffractometer | 2087 independent reflections |
| Radiation source: fine-focus sealed tube | 1773 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.026 |
| Detector resolution: 10.434 pixels mm-1 | θmax = 25.8º |
| T = 295(2) K | θmin = 5.6º |
| φ scans, and ω scans with κ offsets | h = −6→6 |
| Absorption correction: analytical[CrysAlis RED (Oxford Diffraction, 2007). Analytical absorption correction using a multifaceted crystal model based on expressions derived by Clark & Reid (1995)] | k = −9→9 |
| Tmin = 0.852, Tmax = 0.975 | l = −16→16 |
| 23656 measured reflections |