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. 2008 Mar 29;64(Pt 4):o769. doi: 10.1107/S1600536808008155
Oxford Xcalibur diffractometer 2087 independent reflections
Radiation source: fine-focus sealed tube 1773 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.026
Detector resolution: 10.434 pixels mm-1 θmax = 25.8º
T = 295(2) K θmin = 5.6º
φ scans, and ω scans with κ offsets h = −6→6
Absorption correction: analytical[CrysAlis RED (Oxford Diffraction, 2007). Analytical absorption correction using a multifaceted crystal model based on expressions derived by Clark & Reid (1995)] k = −9→9
Tmin = 0.852, Tmax = 0.975 l = −16→16
23656 measured reflections